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HPLC法对硫酸茚地那韦的分析检测
波长：220nm 流速：1.0ml/min
流动相：A:
B:乙腈
A B
0 80 20
40 30 70
45 30 70
47 80 20
52 80 20
色谱柱：琛航色谱柱91182545 C18 5μ 250×4.6 801034
|
Channel A -- Absorbance_ |
|
|
|
|
|
Pk # |
Retention Time |
Area |
Area Percent |
Theoretical plates (USP) |
|
1 |
27.017 |
3686879 |
74.273 |
74658 |
|
2 |
35.167 |
210232 |
4.235 |
13406 |
|
3 |
36.050 |
14985 |
0.302 |
97876 |
|
4 |
38.465 |
343912 |
6.928 |
29083 |
|
5 |
39.750 |
10909 |
0.220 |
103726 |
|
6 |
40.445 |
75455 |
1.520 |
74823 |
|
7 |
41.223 |
360574 |
7.264 |
38856 |
|
8 |
44.373 |
207700 |
4.184 |
16339 |
|
9 |
45.807 |
20733 |
0.418 |
107534 |
|
10 |
47.417 |
32579 |
0.656 |
53773 |
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